ICHRegulatory IntelligenceGuidance
ICH Q11

Development and Manufacture of Drug Substances (Chemical and Biotechnological/Biological Entities)

Provides guidance on the application of QbD concepts to the development and manufacture of drug substances, covering selection of starting materials, control of critical quality attributes, and design space for API processes.

LAST REVISED
May 2012
PRODUCT AREAS
ApiBiotech

What this does not cover

stated in the document's own scope
  • Covers development and manufacture of the drug substance; development of the finished drug product is ICH Q8.
  • Addresses development and CMC content, not the commercial GMP for API manufacture, which is ICH Q7.
  • Covers chemical and biotechnological/biological drug substances, but not the viral-safety evaluation of biotech products, which is ICH Q5A.
  • Describes the control strategy and starting-material justification, not the lifecycle-change tools for later CMC changes, which are ICH Q12.
SOURCE & PROVENANCE
ISSUING BODY
International Council for Harmonisation
JURISDICTION
International
DOCUMENT ID
ICH Q11
Official site — International Council for Harmonisation

Always verify against the current published text before relying on it for a submission or inspection.

Overview

ICH Q11 addresses the development and manufacture of drug substances — the active substance — for both chemical entities and biotechnological/biological entities. It extends the Quality by Design and risk principles of ICH Q8 and Q9 to the API: it explains how to describe the manufacturing process and its controls, how to link material attributes and process parameters to the drug substance’s critical quality attributes, and how to justify the selection of starting materials, which is one of its most consequential topics. It also covers the design space at the drug-substance level and the information that should appear in the drug-substance sections of the marketing application.

Scope & applicability

Drug substance manufacturers for both small molecule APIs and biological/biotechnological entities. Focuses on the chemistry, manufacturing, and controls (CMC) section of regulatory submissions.

Legal basis & how it acquires force

Q11 is an ICH Quality guideline, finalised at Step 4 in May 2012. An ICH guideline is not itself law; regions implement it. The FDA issued Q11 as a guidance for industry, the EMA adopted it as a scientific guideline, and Japan gives it effect through MHLW. It describes the content of the drug-substance sections (3.2.S) of the ICH Common Technical Document used across the regions, so a sponsor meets the regional filing requirement while Q11 supplies the harmonised expectation for what that content should demonstrate.

Document structure

PartCovers
Manufacturing process developmentApplying enhanced (QbD) and traditional approaches to develop the drug-substance process
Selection of starting materialsThe general principles for choosing and justifying starting materials for chemical and biological entities
Control strategyLinking CQAs, material attributes, and process parameters into a drug-substance control strategy
Process validation and design spaceEstablishing a drug-substance design space and the approach to process validation
Submission of information (3.2.S)What to present in the drug-substance sections of the marketing application
Illustrative examples (Annex)Worked examples of starting-material selection for chemical and biotechnological substances

Key requirements

  • Scientific justification for proposed starting material selection
  • Identification of CQAs for the drug substance
  • Development studies establishing critical process parameters
  • Linkage between development work and commercial manufacturing controls

Revision notes

May 2012. No revisions. Q&A document (2017) clarified starting material requirements.

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International alignment

Q11 is the drug-substance counterpart to Q8’s drug-product development, applying the same QbD vocabulary — QTPP, CQAs, design space, control strategy — one level upstream. It relies on the risk method of Q9 and the quality system of Q10, connects to the API GMP guide Q7 for commercial manufacture, and its later Q&A addendum clarified starting-material selection. Its content maps to Module 3 of the ICH CTD used by the FDA, EMA, and PMDA.

ICH Q11: frequently asked questions

Quick answers to common questions about ICH Q11.

What does ICH Q11 cover that ICH Q8 does not?

Q11 applies the Quality by Design and control-strategy concepts to the drug substance (the active), including the selection and justification of starting materials, whereas Q8 covers development of the finished drug product. They are companion guidelines at different points in the process.

Why is starting-material selection so central to ICH Q11?

The chosen starting material defines where GMP and full CMC control begin. Q11 sets general principles for justifying that selection for both chemical and biological entities, and a later Q&A addendum expanded on it, because the decision affects the scope of the control strategy.

Is ICH Q11 legally binding?

Not by itself. It is a harmonised ICH guideline adopted regionally — as FDA guidance, an EMA scientific guideline, and through MHLW in Japan. It describes the drug-substance content of the Common Technical Document.